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(Solved): hexane. Draw line-angle (bond-line) structures of both compounds. b) (1) Circle the more polar compo ...



hexane. Draw line-angle (bond-line) structures of both compounds. b) (1) Circle the more polar compound: ethyl acetate 2. Answer the following questions about the TLC diagrams below. A. 35 mm Sealed TLC chamber with solvent level shown hexane a) (1) For diagram A, state what is wrong with the TLC set-up (assume the slide has been placed inside the TLC chamber). 22 mm b) (1) For diagram B, circle the spot that contains the most non-polar compound. B. 3. (2) A developed TLC plate is shown below. Calculate the Rf of the spot. Show all work. TRUE A B 4. Answer each of the following as True or as False: a. (1) A more polar compound will have a larger R, than a nonpolar one. b) The plate run in 2:1 ethyl acetate:hexanes b) (1) A large R, means a spot travels further up the slide, away from the baseline. FALSE 5. (1) Assume you have a TLC plate with spotted with acetaminophen. Which of the following would have the larger R? value (chose a or b): a) The plate run in 3:2 hexanes:ethyl acetate

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hexane. Draw line-angle (bond-fine) structures of both compounds. b) (1) Circle the more polar compound: ethyl acetate hexane 2. Answer the following questions about the TLC diagrams beiow. a) (1) For diagram A, state what is wrong with the the set-up (assume the slide has been placed inside the ThC chamber). b) (1) For diagram B, circle the spot that contains the most non:polar compound. 3. (2) A developed RC plate is shown below. Calculate the Ru of the spot. Show all work. 4. Answer each of the following as True or as False: a. (1) A more polar compound will have a larger than a nonpolar one. TRNE b) (1) A large R, means a spot travels further up the slide, away from the baseline. TALSE 5. (1) Assume you have a TLC plate with spotted with acetaminophen. Which of the following would have the larger , value (chose a or b): a) The plate run in hexanes ethyl acetate b) The plate run in 2:1 ethyl acetate:hexanes


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